Journal of Electroanalytical Chemistry and Interfacial Electrochemistry
An electroanalytical investigation on the nickel-promoted electrochemical conversion of CO2 to CO
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Electrochemical preparation of standard solutions of Pb(II) ions in ionic liquid for analysis of hydrophobic samples: The olive oil case
2017, TalantaCitation Excerpt :Some decades ago, the problem of preparing anhydrous standard ionic solutions in aprotic organic solvents such as acetonitrile, DMSO, DMF, propylencarbonate etc., was faced by developing relatively easy electrochemical preparation methods [29,30]. It was demonstrated that, by oxidizing a metal anode under controlled anhydrous conditions in the aprotic medium, it was possible to generate metal ion solutions whose concentration could be controlled coulometrically [29,30]. The method showed to be feasible also for preparing with accuracy solutions of anhydrous HClO4 obtained by the electrochemical oxidation of hydrogen gas in pre-dried aprotic solvents, which were successfully used as standards to define an absolute pH scale from proton basicity in aprotic solvents [31,32].
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1998, Inorganica Chimica Acta