In situ waxs-saxs synchrotron study of the kinetics of nucleation and growth in linde type-a zeolite (LTA)
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Real-time inline monitoring of zeolite synthesis by Photon Density Wave spectroscopy
2019, Microporous and Mesoporous MaterialsCitation Excerpt :In the past, efforts to analyze the crystallization of zeolites in real-time have been undertaken on the lab scale with focus on mechanisms rather than particle size. Different analytical methods, such as electrochemical methods/conductivity [10,11], viscosity measurements [12], calorimetry [13], spectroscopic methods [14] (IR [15,16], Raman [17–19], NMR [20,21], X-Ray absorption (XANES, EXAFS) [22]), mass spectrometry [23], and X-ray powder diffraction (XRD) [24–26] as well as X-ray scattering (SAXS, WAXS) [22,27–29], have been employed. To the best of our knowledge, only two publications report on inline spectroscopic methods applicable in pilot or production scale (IR spectroscopy [30], Raman spectroscopy [31]), whereas all others are based on specially designed at-/off-line measurement cells or sampling approaches for zeolite characterization.
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