Issue 6, 2004
From the journal:

Journal of Materials Chemistry

Synthesis and structural characterization of ordered supermicroporous MSU type silica–tin molecular sieves

Manuela Casagrande,a   Loretta Storaro,a   Maurizio Lenarda,*a   Jacopo Gersich,a   Lorenzo Stievano,b   Friedrich E. Wagnerc  and  Tiziana Montanarid  

* Corresponding authors

a INSTM UdR di Venezia, Dipartimento di Chimica, Università Ca' Foscari, Via Torino 155b, Mestre Venezia, Italy
E-mail: lenarda@unive.it
Fax: 0039-041-2346735
Tel: 039-041-2346762

b Laboratoire de Réactivité de Surface UMR 7609, Université Pierre et Marie Curie - Paris VI, Casier 178, 4, Place Jussieu, Paris CEDEX 05, France

c Physik-Department E15, Technische Universität München, Garching, Germany

d INSTM UdR di Genova, Dipartimento di Ingegneria Chimica del Processo, Università di Genova, P.le J.F.Kennedy, Genova

Abstract

Supermicroporous Sn–Si molecular sieves, with different amounts of tin, have been prepared using polyethylene oxide type surfactants as structure directing agents and a silicon alkoxide as precursor. Syntheses have been carried out in acidic media. The structural and chemical properties of the prepared materials, have been studied using a variety of techniques such as Wide Angle X-Ray Scattering (WAXS), physisorption of N2 at 77K, FT-IR spectroscopy of chemisorbed pyridine, skeletal FT-IR, Temperature Programmed Desorption of ammonia (NH3-TPD) and 119Sn Mössbauer spectroscopy.

Graphical abstract: Synthesis and structural characterization of ordered supermicroporous MSU type silica–tin molecular sieves

About
Cited by
Related
Download options Please wait...

Additions and corrections

Article information

DOI
https://doi.org/10.1039/B314259K
Article type
Paper
Submitted
07 Nov 2003
Accepted
19 Jan 2004
First published
16 Feb 2004

J. Mater. Chem., 2004,14, 1010-1016

Permissions

Request permissions

Synthesis and structural characterization of ordered supermicroporous MSU type silica–tin molecular sieves

M. Casagrande, L. Storaro, M. Lenarda, J. Gersich, L. Stievano, F. E. Wagner and T. Montanari, J. Mater. Chem., 2004, 14, 1010 DOI: 10.1039/B314259K

To request permission to reproduce material from this article, please go to the Copyright Clearance Center request page.

If you are an author contributing to an RSC publication, you do not need to request permission provided correct acknowledgement is given.

If you are the author of this article, you do not need to request permission to reproduce figures and diagrams provided correct acknowledgement is given. If you want to reproduce the whole article in a third-party publication (excluding your thesis/dissertation for which permission is not required) please go to the Copyright Clearance Center request page.

Read more about how to correctly acknowledge RSC content.

Spotlight

Advertisements